Readme-Topotactic conversion of Ni3CuN into Ni3Cu with Anti-Perovskite Structure Reveals the Role of Nitrogen on Electrocatalytic Properties Depositor: Alexey Ganin, Zhengxin Yang Date: 26 May 2026 Institution: School of Chemistry, University of Glasgow, University Avenue, Glasgow G12 8QQ, United Kingdom 1. Dataset Overview The raw data on the chronopotentiometry experiments of Ni3CuN and Ni3Cu in 1 M KOH at 50 mA/cm2 for 24 hours have been provided in the Excel file. 2. File Description File name: Chronopotentiometry experiments of Ni3CuN and Ni3Cu.xlsx This Excel workbook contains 1 worksheet named Figure2. ColumnA-B: Chronopotentiometry experiment at -50 mA/cm2 of Ni3CuN for 24 hours ColumnD-E: Chronopotentiometry experiment at -50 mA/cm2 of Ni3Cu for 24 hours 3. Software Requirements File Type: .xlsx Required Software: Microsoft Excel or any software supporting XLSX format Notes: Data are in standard tabular format with labelled columns. 4. Data Description Each sheet contains tabulated data with labelled columns corresponding to the measured variables: X-axis variable: Time(s) Y-axis variable: Potential (V vs. Ag/AgCl in 3.5M KCl) 5. Instrument / Technique Details Chronopotentiometry experiments: EC-Lab Biologic VSP potentiostat Applied current: -50 mA (The working area of the electrode was 1×1cm2) Duration: 24 hours iR compensation of 85%: Yes (Automatic Biologic potentiostat function) 6. Chemicals Used Potassium hydroxide: Potassium hydroxide, ca. 85%, ACS reagent, pellets 7.Contact Information: For further information about this dataset, please contact: Dr. Alexey Y. Ganin alexey.ganin@glasgow.ac.uk WestCHEM, School of Chemistry, University of Glasgow, University Avenue, Glasgow G12 8QQ, United Kingdom