This data belongs to cyclic voltammetry experemient for compound 1F, 2F and 4F [1,4-bis(2-(3,4-ethylene-dioxy)Thienyl)-fluorbenzene]. Cyclic voltammetry experiment for the monomers ca. (0.1 mM) and polymers were prformed using gold and ITO working electrodes. Pt counter electrode and Ag reference electrode were used in dichloromethane and TBAPF6 (0.1 M) as electrolyte at scan rate of 0.1 V/s with sensitivity 10-4 A/V measurements were conducted with iR compensation. The data is referenced to the Fc/Fc+ redox couple.