Data for Manuscript =================== Data for manuscript "Kinetic Control of Interpenetration in Fe–Biphenyl-4,4′-dicarboxylate Metal–Organic Frameworks by Coordination and Oxidation Modulation" Journal of the American Chemical Society 2019 Authors: Dominic Bara Claire Wilson Max Mörtel Marat M. Khusniyarov Sanliang Ling Ben Slater Stephen Sproules Ross S. Forgan Experimental data in Origin format, Bruker NMR format, Avogadro molecular modelling format and images as jpg files RSF thanks the Royal Society for a University Research Fellowship. This project received funding in part from the European Research Council (ERC) under the European Union’s Horizon 2020 Programme for Research and Innovation (grant agreement no. 677289, SCoTMOF, ERC-2015-STG). Via our membership of the UK’s HEC Materials Chemistry Consortium, which is funded by EPSRC (EP/L000202, EP/R029431), this work used the ARCHER UK National Supercomputing Service (http://www.archer.ac.uk). MMK is grateful to the Deutsche Forschungsgemeinschaft (DFG Research Grant KH 279/3) and Emerging Talents Initiative (ETI) program of the FAU Erlangen-Nürnberg for financial support. CCDC 1914373-1914374 contain the supplementary crystallographic data for this work.These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif. Data available NMR spectra, Thermogravimetric analysis, powder X-ray diffraction, nitrogen adsorption, SEM images.