Data for Manuscript =================== Data for manuscript "Controlling Interpenetration Through Linker Conformation in the Modulated Synthesis of Sc Metal–Organic Frameworks” Journal of Materials Chemistry A, 2018 Authors: R. J. Marshall, C. T. Lennon, A. Tao, H. M. Senn, C. Wilson, D. Fairen-Jimenez and R. S. Forgan Experimental data in Origin format, Bruker NMR format and as jpg files Funded by EPSRC grants EP/L004461/1 and ERC grants 677289, SCoTMOF, ERC-2015-STG; 726380, NanoMOFdeli, ERC-2016-COG CCDC 1559284–1559286 contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif. Data available NMR spectra, Thermogravimetric analysis, powder X-ray diffraction, nitrogen adsorption, SEM images and DFT calculations.