Pdf of 1H, 13C, 31P NMR spectra of (3-hydroxypropyl)triphenylphosphonium chloride (LP061), (6-hydroxyhex-1-yl)triphenylphosphonium bromide (LP135), TPP3-malonate (LP117), TPP6-malonate (LP149), TPP11-malonate used in Selective Delivery of Dicarboxylates to Mitochondria by Conjugation to a Lipophilic Cation via a Cleavable Linker and prepared by Laura Pala and Stuart T. Caldwell in the laboratory of Prof. Richard C. Hartley, University of Glasgow.  All raw data and processing files are included in folders labelled LP061, LP135, LP117, and LP149.  The Mestre Nova (Mnova) file is included for TPP11-malonate. The data were acquired on Bruker AVIII 400 and AVIII 500 spectrometers and processed using Bruker Topspin software.